HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 59752954, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Methyloxybenzyl chloride | HCID 69993 | — |
| Reactant | HCID 178420101 | HCID 178420101 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 59752954 | HCID 59752954 | 89% |
Reaction Steps
A mixture of 3-phenyl-1H-pyrazole (1.35 g, 9.36 mmol), 4-methoxybenzyl chloride (1.5 g, 9.7 mmol) and K2CO3 (3.3 g, 24.2 mmol) in methyl ethyl ketone was refluxed for 24 h. The salts were filtered off, and the solvent was removed in vacuo. The residue was purified by a column chromatography on silica gel to yield the title compound (2.2 g, 89%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07402684B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-abfe223b0e704837ae0864d230308a05 |
| Source note | uspto-grants-2008_07 |