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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 750098Generated: October 30, 2026

Potassium Carbonate → HCID 59752954, compound

https://huagongshe.com/reaction/750098

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant4-Methyloxybenzyl chlorideHCID 69993—
ReactantHCID 178420101HCID 178420101—
SolventMethyl Ethyl KetoneHCID 6569—
ProductHCID 59752954HCID 5975295489%

Reaction Steps

A mixture of 3-phenyl-1H-pyrazole (1.35 g, 9.36 mmol), 4-methoxybenzyl chloride (1.5 g, 9.7 mmol) and K2CO3 (3.3 g, 24.2 mmol) in methyl ethyl ketone was refluxed for 24 h. The salts were filtered off, and the solvent was removed in vacuo. The residue was purified by a column chromatography on silica gel to yield the title compound (2.2 g, 89%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07402684B2
Source datasetuspto-grants-2008_07
ORD IDord-abfe223b0e704837ae0864d230308a05
Source noteuspto-grants-2008_07