Furfural → HCID 69156316, compound
Reaction equation
[CH3:1][O:2][C:3]([C:5]1[N:6]([NH2:23])[C:7](=[O:22])[C:8]2[C:13]([C:14]=1[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)=[CH:12][C:11]([Cl:21])=[CH:10][CH:9]=2)=[O:4].[O:24]1[CH:28]=[CH:27][CH:26]=[C:25]1[CH:29]=O>>[CH3:1][O:2][C:3]([C:5]1[N:6]([N:23]=[CH:29][C:25]2[O:24][CH:28]=[CH:27][CH:26]=2)[C:7](=[O:22])[C:8]2[C:13]([C:14]=1[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)=[CH:12][C:11]([Cl:21])=[CH:10][CH:9]=2)=[O:4]Participants
3
Procedure
The present compound was synthesized by a method similar to that in Example 210 and using 2-amino-6-chloro-1-oxo-4-phenyl-1,2-dihydroisoquinoline-3-carboxylic acid methyl ester (210 mg) and furan-2-carbaldehyde. A colorless powder (125 mg).
Workup
- customThe present compound was synthesized by a method similar to that in Example 210
Sources & evidence
- ORD record
- ord-9cefda8817be45bf9830e418cd47eb21
- Source dataset
- uspto-grants-2008_07
- Patent number
- US07402595B2
Reaction notes
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