Acetic Acid Mixture with Hydrobromic Acid → HCID 10127499, compound

Participants

Reaction Steps

25% Hydrogen bromide-acetic acid solution (10.0 ml) was added to [2-(benzo[1,3]dioxol-5-ylmethyl)-6-bromo-1-oxo-4-phenyl-1,2-dihydroisoquinolin-3-yl]carbamic acid benzyl ester (3.6 g), and the mixture was stirred at room temperature for 1 hr. The precipitate was collected by filtration, washed with diethyl ether and dried to give the title compound (3.3 g) as a colorless powder.

Provenance & Evidence