3-Formylphenylboronic acid → HCID 86599561, compound

HRID 750284Notes

Reaction equation

HRID 750284 reaction equation
[CH3:1][O:2][C:3]([C:5]1[N:6]([CH2:25][C:26]2[CH:31]=[CH:30][C:29]([C:32]([O:34][CH3:35])=[O:33])=[CH:28][CH:27]=2)[C:7](=[O:24])[C:8]2[C:13]([C:14]=1OS(C(F)(F)F)(=O)=O)=[CH:12][C:11]([Cl:23])=[CH:10][CH:9]=2)=[O:4].[CH:36]([C:38]1[CH:39]=[C:40](B(O)O)[CH:41]=[CH:42][CH:43]=1)=[O:37]>>[CH3:1][O:2][C:3]([C:5]1[N:6]([CH2:25][C:26]2[CH:27]=[CH:28][C:29]([C:32]([O:34][CH3:35])=[O:33])=[CH:30][CH:31]=2)[C:7](=[O:24])[C:8]2[C:13]([C:14]=1[C:42]1[CH:41]=[CH:40][CH:39]=[C:38]([CH:36]=[O:37])[CH:43]=1)=[CH:12][C:11]([Cl:23])=[CH:10][CH:9]=2)=[O:4]

Participants

3

Reactant 2

HCID 27343563-Formylphenylboronic acidHCID 86599562HCID 86599562, compound

Product 1

HCID 86599561HCID 86599561, compound

Procedure

The present compound was synthesized by a method similar to that in Example 272 and using 6-chloro-2-(4-methoxycarbonylbenzyl)-1-oxo-4-trifluoromethanesulfonyloxy-1,2-dihydroisoquinoline-3-carboxylic acid methyl ester and 3-formylphenylboronic acid.

Workup

  1. customThe present compound was synthesized by a method similar to that in Example 272

Sources & evidence

ORD record
ord-ebd87e9768864814bc85a97b20726617
Source dataset
uspto-grants-2008_07
Patent number
US07402595B2

Reaction notes

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