HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonate → HCID 23060531, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonate | HCID 85257 | — |
| Reactant | Sodium methanethiolate | HCID 4378561 | — |
| Reactant | HCID 23060581 | HCID 23060581 | — |
| Product | HCID 23060531 | HCID 23060531 | 64% |
Reaction Steps
By a method similar to that in Example 395, 3-acetyl-6-bromo-2-(4-hydroxymethylbenzyl)-4-phenyl-2H-isoquinolin-1-one was converted to mesylate and reacted with sodium thiomethoxide to give the title compound (239 mg, 64%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07402595B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-52038a8df00042028f039c1360c4b3aa |
| Source note | uspto-grants-2008_07 |