HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Difluorobenzaldehyde → HCID 59753876, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Difluorobenzaldehyde | HCID 136284 | — |
| Reactant | 5-Bromo-2,4-dichloropyrimidine | HCID 289973 | — |
| Product | HCID 59753876 | HCID 59753876 | 88% |
Reaction Steps
The compound was prepared from 5-bromo-2,4-dichloropyrimidine (Aldrich) and 2,6-difluorobenzaldehyde (Aldrich) in 88% yield in an analogous manner as described in Example 1. 1H NMR (300 MHz, CDCl3) δ 9.09 (s, 1H), 7.35 (m, 1H, 7.92 (m, 2H), 6.35 (s, 1H), 2.67 (br. s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07405220B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-ea278d0d532946d399bf4e075fbb1fbe |
| Source note | uspto-grants-2008_07 |