HuagongsheHuagongshe Chemistry Print Report · For research reference only
[1-(Methylsulfonyl)piperidin-4-yl]amine trifluoroacetate → HCID 178504945, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | [1-(Methylsulfonyl)piperidin-4-yl]amine trifluoroacetate | HCID 11975076 | — |
| Reactant | HCID 178478328 | HCID 178478328 | — |
| Product | HCID 178504945 | HCID 178504945 | 21% |
Reaction Steps
The compound was prepared from 6-chloro-3-phenyl-1H-pyrazolo[3,4-d]pyrimidine (Example 14) and 1-methanesulfonyl-piperidin-4-ylamine; compound with trifluoro-acetic acid in an analogous manner as described in Example 4 and was purified by HPLC (Gilson) to give a free base (21% yield). MS (M+H)+, 373.24.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07405220B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-25f8dfa3e484433dbe136023afb15cc4 |
| Source note | uspto-grants-2008_07 |