HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Bromide → HCID 86590082, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Bromide | HCID 6323 | — |
| Reactant | HCID 86590083 | HCID 86590083 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86590082 | HCID 86590082 | — |
Reaction Steps
0.6 g (0.002 mol) 4f are taken up in 20 mL acetonitrile and reacted with 1.14 g (0.006 mol) of 50% methyl bromide solution in acetonitrile analogously to step 1.3. Yield: 0.44 g beige crystals (45% of theoretical yield); melting point: 227° C.-228° C.; elemental analysis: calculated: C (58.55), H (4.91), N (2.84); found: C (57.19), H (5.11), N (2.86).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07405224B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-f192ff41bb8c4c45b9fb5cadd57cee8d |
| Source note | uspto-grants-2008_07 |