HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chlorophenol → HCID 59753891, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chlorophenol | HCID 7933 | — |
| Reactant | HCID 69198607 | HCID 69198607 | — |
| Product | HCID 59753891 | HCID 59753891 | — |
Reaction Steps
2-Methylsulfonyl-4-(2,4-dichlorophenyl)-5-(4-chlorophenyl)pyrimidine from Reference Example 3 was reacted with 3-chlorophenol according to the procedure described in Example 74 to afford 2-(3-chlorophenyloxy)-4-(2,4-dichlorophenyl)-5-(4-chlorophenyl)pyrimidine: HPLC/MS: m/e=461 (M++1); Rt=4.72 min; 1H-NMR 400 MHz (CDCl3): δ 7.00-7.12. (m, 2H), 7.11-7.18 (m, 2H), 7.20-7.30 (m, 7H), 8.60 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07405221B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-72ef9bbfc72c40138aae1db19af93817 |
| Source note | uspto-grants-2008_07 |