HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Pentyn-1-ol → 4-Pentyn-1-ol, 5-[3-(trifluoromethoxy)phenyl]-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Pentyn-1-ol | HCID 79346 | — |
| Reactant | 1-Iodo-3-(trifluoromethoxy)benzene | HCID 2777293 | — |
| Catalyst | HCID 178418397 | HCID 178418397 | — |
| Product | 4-Pentyn-1-ol, 5-[3-(trifluoromethoxy)phenyl]- | HCID 68821693 | — |
Reaction Steps
In analogy to the procedure described in example 1 a], 1-iodo-3-trifluoromethoxy-benzene was reacted with 4-pentyn-1-ol in the presence of Pd(PPh3)4 and cuprous iodide to give the title compound as red oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07405236B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-2a7ce73c88bc42b3accbfa0c14609e2e |
| Source note | uspto-grants-2008_07 |