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HRID751214

反应详情

EQUATION

反应方程式

HRID 751214 的结构方程式

REACTANTS

反应物

3
结构：CCOC(=O)CBr
HCID7748

Ethyl bromoacetate

C4H7BrO2

结构：O=C([O-])[O-].[Cs+].[Cs+]
HCID10796

Cesium carbonate

CCs2O3

结构：CC(C)(C)[Si](C)(C)Oc1cccc2cc[nH]c12
HCID57110974

7-[[(1,1-Dimethylethyl)dimethylsilyl]oxy]-1H-indole

C14H21NOSi

PRODUCTS

生成物

1
结构：CCOC(=O)Cn1ccc2cccc(O[Si](C)(C)C(C)(C)C)c21
HCID68824002

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

In analogy to the procedure described in example 6 b], 7-(tert-butyl-dimethyl-silanyloxy)-1H-indole (EP 206225 A2) was reacted with ethyl bromoacetate in the presence of cesium carbonate in acetonitrile to give the title compound as colorless liquid.