HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 178492419, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178501502 | HCID 178501502 | — |
| Solvent | Methanol--water (1/1) | HCID 22242641 | — |
| Product | HCID 178492419 | HCID 178492419 | — |
Reaction Steps
Operating mode: 1 equivalent of N-(4-methoxyphenylazoformyl)L-phenylalanine arginine methyl ester was taken up in a water/methanol mixture (ratio: 1/2; 3 ml/mmol). 3 equivalent of 1 N sodium hydroxide was added. After 1 h, the reactional medium was acidified, concentrated then extracted with water/dichloromethane. The dichioromethane phase was evaporated then dried. N-(4-methoxyphenylazoformyl)-L-phenylalanyl arginine was obtained as an orange powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07405280B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-e17b668793fc448c91a392414d4c53e0 |
| Source note | uspto-grants-2008_07 |