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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 751338Generated: October 31, 2026

Azepane → HCID 59754753, compound

https://huagongshe.com/reaction/751338

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAzepaneHCID 8119—
Reactant2-chloro-1-phenyl-1H-indole-3-carbaldehydeHCID 314793—
ProductHCID 59754753HCID 5975475342%

Reaction Steps

2-Chloro-1-phenyl-1H-indole-3-carboxaldehyde is reacted with azepane as described in Example 2 to give the title compound (42% yield). NMR (CDCl3) 10.25 (1H, s), 8.23 (1H, d), 7.58 (2H, m), 7.51 (1H, m), 7.39 (2H, d), 7.25 (1H, m), 7.15 (1H, t), 6.98 (1H, d), 3.50 (4H, m), 2.55 (4H, m), 2.33 (3H, s), 1.78 (2H, m).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07405300B2
Source datasetuspto-grants-2008_07
ORD IDord-1742bd4f6b734b12a029a4626a111568
Source noteuspto-grants-2008_07