HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azepane → HCID 59754753, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azepane | HCID 8119 | — |
| Reactant | 2-chloro-1-phenyl-1H-indole-3-carbaldehyde | HCID 314793 | — |
| Product | HCID 59754753 | HCID 59754753 | 42% |
Reaction Steps
2-Chloro-1-phenyl-1H-indole-3-carboxaldehyde is reacted with azepane as described in Example 2 to give the title compound (42% yield). NMR (CDCl3) 10.25 (1H, s), 8.23 (1H, d), 7.58 (2H, m), 7.51 (1H, m), 7.39 (2H, d), 7.25 (1H, m), 7.15 (1H, t), 6.98 (1H, d), 3.50 (4H, m), 2.55 (4H, m), 2.33 (3H, s), 1.78 (2H, m).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07405300B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-1742bd4f6b734b12a029a4626a111568 |
| Source note | uspto-grants-2008_07 |