Hydrogen Peroxide → HCID 69268667, compound

Participants

Reaction Steps

Dissolve (1H-indol-3-yl)acetonitrile (3.40 mmol) in dry dimethyl sulfoxide (3.0 mL), cool in an ice bath, combine with anhydrous potassium carbonate (0.200 g) and 30% hydrogen peroxide (0.6 mL), keeping the reaction temperature below 20° C. Warm to room temperature, add water (10 mL) and filter the resulting solid, dry under vacuum.

Provenance & Evidence