HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Fluorophenethylamine → HCID 11267105, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Fluorophenethylamine | HCID 4653 | — |
| Reactant | 5-chloro-1H-pyrrolo[2,3-c]pyridine-2-carboxylic acid | HCID 44630704 | — |
| Product | HCID 11267105 | HCID 11267105 | — |
Reaction Steps
The title compound was prepared as outlined in EXAMPLE 1 from 5-chloro-1H-pyrrolo[2,3-c]pyridine-2-carboxylic acid (Preparation 18) and 4-fluorophenethylamine. The product was purified by mass directed purification to give the title compound as an orange solid. δH (CD3OD): 2.93 (2H, t), 3.60 (2H, t), 6.97–7.04 (3H, m), 7.24–7.30 (2H, m), 7.65 (1H, s), 8.56 (1H, s); m/z (ES+)=318 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07405210B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-5083e88e2ae14db1a6bb9c2ef9aea485 |
| Source note | uspto-grants-2008_07 |