HCID 59753324, compound → HCID 59753350, compound

Participants

Reaction Steps

A solution of 10.00 g (20.51 mmol) of the ester from example 22A in methanol (100 ml) is treated with Pd/C (1.00 g) (10 pc.) and hydrogenated at RT at a hydrogen pressure of 1 bar. Subsequently, the solution is filtered through silica gel and evaporated. 7.93 g (97% of th.) of the product are obtained, which is reacted without further purification.

Provenance & Evidence