HRID75505

反应详情

EQUATION

反应方程式

HRID 75505 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Trans-[4-(3,5-Diethyl-pyrazol-1-ylmethyl)-cyclohexyl]-carbamic acid tert-butyl ester (80 mg, 0.24 mmol) was dissolved in MeOH (1 ml). 4M HCl/dioxan (1 ml) was added and the RM was stirred at RT for 2 hours. The solvent was removed in vacuo to afford the title product which was used without further purification; LC-MS Rt 1.59 mins [M+H]+ 236.

WORKUP

后处理

  1. customThe solvent was removed in vacuo