HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → HCID 178436377, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 178436379 | HCID 178436379 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178436377 | HCID 178436377 | — |
Reaction Steps
Trans-[4-(3,5-Diethyl-pyrazol-1-ylmethyl)-cyclohexyl]-carbamic acid tert-butyl ester (80 mg, 0.24 mmol) was dissolved in MeOH (1 ml). 4M HCl/dioxan (1 ml) was added and the RM was stirred at RT for 2 hours. The solvent was removed in vacuo to afford the title product which was used without further purification; LC-MS Rt 1.59 mins [M+H]+ 236.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08835444B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-ee3ce2ad3a124c4b968b9d7a7536f624 |
| Source note | uspto-grants-2014_09 |