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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 75505Generated: October 30, 2026

1,4-Dioxane hydrochloride → HCID 178436377, compound

https://huagongshe.com/reaction/75505

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,4-Dioxane hydrochlorideHCID 20443148—
ReactantHCID 178436379HCID 178436379—
SolventMethanolHCID 887—
ProductHCID 178436377HCID 178436377—

Reaction Steps

Trans-[4-(3,5-Diethyl-pyrazol-1-ylmethyl)-cyclohexyl]-carbamic acid tert-butyl ester (80 mg, 0.24 mmol) was dissolved in MeOH (1 ml). 4M HCl/dioxan (1 ml) was added and the RM was stirred at RT for 2 hours. The solvent was removed in vacuo to afford the title product which was used without further purification; LC-MS Rt 1.59 mins [M+H]+ 236.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08835444B2
Source datasetuspto-grants-2014_09
ORD IDord-ee3ce2ad3a124c4b968b9d7a7536f624
Source noteuspto-grants-2014_09