HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → 7-(1-Benzoyl-4-piperidinyl)-5-ethyl-2-phenylimidazo[5,1-f][1,2,4]triazin-4(3H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 5-ethyl-2-phenyl-7-(4-piperidinyl)imidazo[5,1-f][1,2,4]triazin-4(3H)-one | HCID 135752610 | — |
| Product | 7-(1-Benzoyl-4-piperidinyl)-5-ethyl-2-phenylimidazo[5,1-f][1,2,4]triazin-4(3H)-one | HCID 135752673 | — |
Reaction Steps
In analogy to the procedure for Example 103 Step (b), 30 mg (0.09 mmol) 5-ethyl-2-phenyl-7-(4-piperidinyl)imidazo[5,1-f][1,2,4]triazin-4(3H)-one, 14 mg (0.10 mmol) benzoyl chloride are stirred at room temperature overnight, proportionate amounts of the solvents are used.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07087605B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-c29c2191c2d443639bf07ca2ce43a00d |
| Source note | uspto-grants-2006_08 |