Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-(1-(4-Iodophenyl)propan-2-YL)acetamide → 4-Iodo-alpha-methylbenzeneethanamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-(1-(4-Iodophenyl)propan-2-YL)acetamide | HCID 66611344 | — |
| 용매 | Hydrochloric Acid | HCID 313 | — |
| 생성물 | 4-Iodo-alpha-methylbenzeneethanamine | HCID 123870 | — |
반응 단계
9.00 g (29.69 mmol) N-[2-(4-iodo-phenyl)-1-methyl-ethyl]-acetamide (I52.1) are added to 150 mL HCl (4N) and the reaction mixture is stirred at reflux over night. Then the mixture is diluted with soda lye and extracted with EtOAc. The organic layer is dried with Na2SO4 and the solvent is removed in vacuo.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08835472B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-6972a19953ff4a0ca677f361275db46a |
| 출처 메모 | uspto-grants-2014_09 |