HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 77080Erstellt: 25. Oktober 2026
N-(2-Amino-5-chloro-phenyl)-5-bromo-2-fluoro-benzamide → HCID 178505483, Verbindung
https://huagongshe.com/reaction/77080
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
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| Edukt | N-(2-Amino-5-chloro-phenyl)-5-bromo-2-fluoro-benzamide | HCID 24699699 | — |
| Lösungsmittel | Acetic Acid | HCID 176 | — |
| Produkt | HCID 178505483 | HCID 178505483 | 93% |
Reaktionsschritte
Method 7—Step b A mixture of N-(2-Amino-5-chloro-phenyl)-5-bromo-2-fluoro-benzamide (1.60 g, 4.67 mmol) in acetic acid (10 mL) was heated at 85° C. overnight. Solvent was removed under reduced pressure and the solid obtained was washed with dichloromethane and dried to obtain 1.40 g of the title compound (93%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US08835648B2 |
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| Quelldatensatz | uspto-grants-2014_09 |
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| ORD ID | ord-3c482643c6b54f34b682f4dfcc5ca817 |
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| Quellennotiz | uspto-grants-2014_09 |
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