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HRID77418

反应详情

EQUATION

反应方程式

HRID 77418 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc(CNCC2CCOCC2)cc1
HCID55211610

未命名化合物

结构：CC(C)(C)OC(=O)N[C@H]1CCc2cc(C(=O)O)ccc2C1
HCID66663497

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(CN(CC2CCOCC2)C(=O)c2ccc3c(c2)CC[C@H](NC(=O)OC(C)(C)C)C3)cc1
HCID66663601

未命名化合物

PROCEDURE

实验过程

According to method G, (S)-6-tert-butoxycarbonylamino-5,6,7,8-tetrahydronaphthalene-2-carboxylic acid was reacted with (4-methoxybenzyl)(tetrahydropyran-4-ylmethyl)amine. The crude product was purified by chromatography on silica gel (eluent: 30% n-heptane in ethyl acetate). The product was thus obtained with the molecular weight of 508.66 (C30H40N2O5); MS (ESI): 509 (M+H+).

WORKUP

后处理

  1. customThe crude product was purified by chromatography on silica gel (eluent: 30% n-heptane in ethyl acetate)
  2. customThe product was thus obtained with the molecular weight of 508.66 (C30H40N2O5)