N-(4-Methoxybenzyl)-1-(tetrahydro-2H-pyran-4-yl)methanamine → {(S)-6-[(4-Methoxybenzyl)(tetrahydropyran-4-ylmethyl)carbamoyl]-1,2,3,4-tetrahydro-naphthalen-2-yl}carbamic acid tert-butyl ester

Beteiligte Stoffe

Reaktionsschritte

According to method G, (S)-6-tert-butoxycarbonylamino-5,6,7,8-tetrahydronaphthalene-2-carboxylic acid was reacted with (4-methoxybenzyl)(tetrahydropyran-4-ylmethyl)amine. The crude product was purified by chromatography on silica gel (eluent: 30% n-heptane in ethyl acetate). The product was thus obtained with the molecular weight of 508.66 (C30H40N2O5); MS (ESI): 509 (M+H+).

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