HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2-Formyl-5-(trifluoromethyl)benzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Formyl-5-(trifluoromethyl)benzoic acid | HCID 86640859 | — |
| Product | 2-Formyl-5-(trifluoromethyl)benzoyl chloride | HCID 87114033 | — |
Reaction Steps
A solution of Example 375A (0.6 g) and thionyl chloride (3.27 g, 27.5 mmol) was refluxed for 2 hr. The reaction solution was cooled to room temperature, concentrated, azeotroped with toluene, and used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08841334B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-3ccb49dfcfe84c628b4d5ddde61629b1 |
| Source note | uspto-grants-2014_09 |