Diethylamine → HCID 9967177, compound

HRID 7944Notes

Reaction equation

HRID 7944 reaction equation
[CH2:1]([N:5]1[C:10](=[O:11])[C:9]([CH2:12]OS(C)(=O)=O)=[CH:8][C:7]([C:18]2[CH:23]=[CH:22][C:21]([CH3:24])=[CH:20][CH:19]=2)=[N:6]1)[CH:2]([CH3:4])[CH3:3].[CH2:25]([NH:27][CH2:28][CH3:29])[CH3:26]>>[CH2:25]([N:27]([CH2:12][C:9]1[C:10](=[O:11])[N:5]([CH2:1][CH:2]([CH3:4])[CH3:3])[N:6]=[C:7]([C:18]2[CH:23]=[CH:22][C:21]([CH3:24])=[CH:20][CH:19]=2)[CH:8]=1)[CH2:28][CH3:29])[CH3:26]

Participants

3

Reactant 2

HCID 8021DiethylamineHCID 219915892-isobutyl-4-methanesulfonyloxymethyl-6-(4-methylphenyl)-2H-pyridazin-3-one2×

Product 1

HCID 9967177HCID 9967177, compoundYield 95%

Procedure

Following the procedure of Example 9 (4), 2-isobutyl-4-methanesulfonyloxymethyl-6-(4-methylphenyl)-2H-pyridazin-3-one and diethylamine were reacted to yield the title compound as a pale yellow oil (yield: 95.0%).

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-3a3c9318f6ac4f7f9a67a326862e69ad
Source dataset
uspto-grants-2006_08
Patent number
US07087606B2

Reaction notes

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