Methanol → 9-Chloro-4-methyl-3,4,5,6-tetrahydro-1H-benzo[e][1,4]diazocin-2-one

HRID 801966Notes

Reaction equation

HRID 801966 reaction equation
[CH2:21]1[CH2:22][CH2:23][CH:24]([N:25]=[C:26]=[N:27][CH:28]2[CH2:29][CH2:30][CH2:31][CH2:32][CH2:33]2)[CH2:34][CH2:35]1.[CH3:36][OH:37].[Cl:1][c:2]1[cH:3][c:4]([N+:16]([O-:17])=[O:18])[c:5]([CH2:8][CH2:9][N:10]([CH3:11])[CH2:12][C:13](=[O:14])[OH:15])[cH:6][cH:7]1.[H:19][H:20].[Pt:38]>>[Cl:1][c:2]1[cH:3][c:4]2[c:5]([cH:6][cH:7]1)[CH2:8][CH2:9][N:10]([CH3:11])[CH2:12][C:13](=[O:14])[NH:16]2

Participants

6

Reactant 5

HCID 887MethanolHCID 10868DicyclohexylcarbodiimideHCID 23939PlatinumHCID 22236587{[2-(4-chloro-2-nitro-phenyl)-ethyl]-methyl-amino}-acetic AcidHCID 178418361HCID 178418361, compound

Product 1

HCID 222365829-Chloro-4-methyl-3,4,5,6-tetrahydro-1H-benzo[e][1,4]diazocin-2-one

Sources & evidence

ORD record
ord-e21886eb361f49d89ce1646618973ec9
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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