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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 80414Generated: October 29, 2026

HCID 68178824, compound → HCID 68178774, compound

https://huagongshe.com/reaction/80414

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68178824HCID 68178824—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 68178774HCID 68178774—

Reaction Steps

To a solution of 40 mg of the compound of step 1.3 (0.068 mmol) in MeOH (2 mL) was added 10% Pd on carbon catalyst (10 mg) and the mixture was vigorously stirred under a hydrogen atmosphere (1 atm) at room temperature for 4 h. After filtration and lyophilization, the titled compound was obtained as a colorless solid (16 mg, 98%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08846645B2
Source datasetuspto-grants-2014_09
ORD IDord-5a6f9d42fb90485f956684be2b831813
Source noteuspto-grants-2014_09