HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68178824, compound → HCID 68178774, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68178824 | HCID 68178824 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68178774 | HCID 68178774 | — |
Reaction Steps
To a solution of 40 mg of the compound of step 1.3 (0.068 mmol) in MeOH (2 mL) was added 10% Pd on carbon catalyst (10 mg) and the mixture was vigorously stirred under a hydrogen atmosphere (1 atm) at room temperature for 4 h. After filtration and lyophilization, the titled compound was obtained as a colorless solid (16 mg, 98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08846645B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-5a6f9d42fb90485f956684be2b831813 |
| Source note | uspto-grants-2014_09 |