Sodium ion → Diethyl-4-(3-azidopropoxy)-2,6-pyridinedicarboxylate

HRID 805100Notes

Reaction equation

HRID 805100 reaction equation
[CH2:10]([CH3:11])[O:12][C:13](=[O:14])[c:15]1[n:16][c:17]([C:22](=[O:23])[O:24][CH2:25][CH3:26])[cH:18][c:19]([Br:21])[cH:20]1.[H-:9].[N:1](=[N+:2]=[N-:3])[CH2:4][CH2:5][CH2:6][OH:7].[Na+:8].[O:27]=[CH:28][N:29]([CH3:30])[CH3:31]>>[N:1](=[N+:2]=[N-:3])[CH2:4][CH2:5][CH2:6][O:7][c:19]1[cH:18][c:17]([C:22](=[O:23])[O:24][CH2:25][CH3:26])[n:16][c:15]([C:13]([O:12][CH2:10][CH3:11])=[O:14])[cH:20]1

Participants

6

Reactant 5

HCID 923Sodium ionHCID 6228DimethylformamideHCID 166653HydrideHCID 109969743-Azidopropan-1-olHCID 13794409Diethyl 4-bromopyridine-2,6-dicarboxylate

Product 1

HCID 22323654Diethyl-4-(3-azidopropoxy)-2,6-pyridinedicarboxylate

Sources & evidence

ORD record
ord-d39447473fe84dadbdf799d780b03fff
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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