HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178448360, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Toluene | HCID 1140 | — |
| Reactant | HCID 178448359 | HCID 178448359 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 178448360 | HCID 178448360 | 87.3% |
Reaction Steps
To the compound 21 (16 mg), 1 M hydrochloric acid in acetic acid solution was added, and the mixture was stirred at room temperature for 4 hours. To the reaction solution, toluene (5 ml) was added and the precipitated solid was collected by filtration to obtain the title compound (12.7 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08846660B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-fcd5ed3f568e4cf29d9b2b1918b3a1ac |
| Source note | uspto-grants-2014_09 |