Hydrochloric Acid → HCID 178448364, compound

Participants

Reaction Steps

To the compound 102 (1.10 g) in an acetonitrile (44 ml) solution, a 4M hydrochloric acid in ethyl acetate solution (1.5 ml) was added, and the mixture was stirred at room temperature for 5 hours. The precipitated crystals were collected by filtration to obtain the title compound (1.03 g) as a colorless crystal.

Provenance & Evidence