HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178418287, compound → HCID 178461263, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Reactant | HCID 178461264 | HCID 178461264 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178461263 | HCID 178461263 | — |
Reaction Steps
To a solution of trans-(4-methylcyclohexyl)methanol (160 g, 1.25 mol) in DCM (1500 mL) was added pyridinium chlorochromate (405 g, 1.88 mol) at 0° C., and the mixture was stirred at room temperature for 2 h. It was filtered and the filtrate was concentrated in vacuo to give trans-4-methylcyclohexanecarbaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08846657B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-6136ad9f4ef64a878dad3fcff1b70526 |
| Source note | uspto-grants-2014_09 |