HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 55285125, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 58522509 | HCID 58522509 | — |
| Product | HCID 55285125 | HCID 55285125 | — |
Reaction Steps
Tert-butyl((3R,4R)-3-methoxy-1-methyl-piperidin-4-yl)-carbamate (3.01 g) is combined with HCl (4 molar in dioxane, 25 mL). After 1 h the reaction mixture is freed from the solvent in vacuo and used in the next step without any further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08846689B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-b1c6daa410044df38f2e64041c452c3a |
| Source note | uspto-grants-2014_09 |