HRID81508

反应详情

EQUATION

反应方程式

HRID 81508 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

98 mg of tert-butyl {4-[5-(trans-2-fluorocyclohexyloxy)-7-propoxyoxazolo[5,4-d]pyrimidin-2-yl]-2,6-dimethylphenoxy}acetate were dissolved in 3.5 ml of dichloromethane, and treated with 1.5 ml of trifluoroacetic acid. After 16 h, the mixture was concentrated and freeze-dried. This gave 96 mg of the title compound.

WORKUP

后处理

  1. concentrationthe mixture was concentrated
  2. customfreeze-dried