Methanol → 5-Methyl-1-phenylpyrazole-3-carbaldehyde

HRID 816742Notes

Reaction equation

HRID 816742 reaction equation
[CH2:1]([O:3][C:4](=[O:2])[c:6]1[n:7][n:8](-[c:12]2[cH:13][cH:14][cH:15][cH:16][cH:17]2)[c:9]([CH3:11])[cH:10]1)[CH3:5].[CH2:30]([Cl:31])[Cl:32].[CH3:18][CH:19]([CH2:20][AlH:21][CH2:22][CH:23]([CH3:24])[CH3:25])[CH3:26].[CH3:27][OH:28].[OH2:29]>>[O:3]=[CH:4][c:6]1[n:7][n:8](-[c:12]2[cH:13][cH:14][cH:15][cH:16][cH:17]2)[c:9]([CH3:11])[cH:10]1

Participants

6

Reactant 5

HCID 887MethanolHCID 962WaterHCID 6344DichloromethaneHCID 14487Diisobutylaluminum hydrideHCID 10900438Ethyl 5-methyl-1-phenyl-1H-pyrazole-3-carboxylate

Product 1

HCID 141352365-Methyl-1-phenylpyrazole-3-carbaldehyde

Sources & evidence

ORD record
ord-b7776a6e53094f01b413f03d2e8f85e9
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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