Chloroform → 6-Bromo-2,2,7-trimethyl-4H-benzo[1,4]oxazin-3-one

HRID 818607Notes

Reaction equation

HRID 818607 reaction equation
[CH3:1][C:2]1([CH3:14])[O:3][c:4]2[c:5]([cH:9][cH:10][c:11]([CH3:13])[cH:12]2)[NH:6][C:7]1=[O:8].[CH:28]([Cl:29])([Cl:30])[Cl:31].[O:15]=[CH:16][N:17]([CH3:18])[CH3:19].[O:20]=[C:21]1[N:22]([Br:27])[C:23](=[O:24])[CH2:25][CH2:26]1>>[CH3:1][C:2]1([CH3:14])[O:3][c:4]2[c:5]([cH:9][c:10]([Br:27])[c:11]([CH3:13])[cH:12]2)[NH:6][C:7]1=[O:8]

Participants

5

Reactant 4

HCID 6212ChloroformHCID 6228DimethylformamideHCID 67184N-bromobutanimideHCID 594182682,2,7-Trimethyl-2H-benzo[b][1,4]oxazin-3(4H)-one

Product 1

HCID 685856146-Bromo-2,2,7-trimethyl-4H-benzo[1,4]oxazin-3-one

Sources & evidence

ORD record
ord-b6bae32ea0c744ba94d0ff3110c6c355
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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