Dimethylformamide → Methyl 4-(2-amino-2-oxoethoxy)-2-methoxybenzoate

HRID 819221Notes

Reaction equation

HRID 819221 reaction equation
[Br:1][CH2:2][C:3](=[O:4])[NH2:5].[C:11](=[O:12])([O-:13])[O-:14].[Cl:30][CH2:31][Cl:32].[Cs+:15].[Cs+:16].[O:6]=[CH:7][N:8]([CH3:9])[CH3:10].[OH:17][c:18]1[cH:19][c:20]([O:28][CH3:29])[c:21]([C:22](=[O:23])[O:24][CH3:25])[cH:26][cH:27]1>>[CH2:2]([C:3](=[O:4])[NH2:5])[O:17][c:18]1[cH:19][c:20]([O:28][CH3:29])[c:21]([C:22](=[O:23])[O:24][CH3:25])[cH:26][cH:27]1

Participants

7

Reactant 6

HCID 6228DimethylformamideHCID 6344DichloromethaneHCID 19660Carbonate IonHCID 696322-BromoacetamideHCID 104967Cesium cation2×HCID 12532676Methyl 4-hydroxy-2-methoxybenzoate

Product 1

HCID 67211435Methyl 4-(2-amino-2-oxoethoxy)-2-methoxybenzoate

Sources & evidence

ORD record
ord-dee1965138664174befddec0b32f876a
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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