HCID 67076225, compound → HCID 86653100, compound

Participants

Reaction Steps

To a solution of N-(2,6-diethylphenyl)-8-{[4-(hydroxymethyl)-2-methoxyphenyl]amino}-1-methyl-4,5-dihydro-1H-pyrazolo[4,3-h]quinazoline-3-carboxamide (50 mg, 0.097 mmol) in 1 ml of dry DCM, MnO2 (68 mg, 0.78 mmol) was added. The mixture was stirred at room temperature for 5 h, MnO2 filtered off and the solvent removed in vacuo affording the title compound in 80% yield.

Provenance & Evidence