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HRID82160

反应详情

EQUATION

反应方程式

HRID 82160 的结构方程式

REACTANTS

反应物

2
结构：CON(C)C(=O)c1cncc(Br)c1
HCID18472269

5-Bromo-N-methoxy-N-methylpyridine-3-carboxamide

C8H9BrN2O2

结构：CC(C)(CO[Si](C)(C)C(C)(C)C)n1cc(I)c2cnc(Cl)nc21
HCID86672084

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(CO[Si](C)(C)C(C)(C)C)n1cc(C(=O)c2cncc(Br)c2)c2cnc(Cl)nc21
HCID86672086

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to the method described for Preparation 28 using 7-(2-{[tert-butyl(dimethyl)silyl]oxy}-1,1-dimethylethyl)-2-chloro-5-iodo-7H-pyrrolo[2,3-d]pyrimidine (see Preparation 44) and 5-bromo-N-methoxy-N-methylnicotinamide to afford the title compound as a yellow solid in 42% yield, 1.40 g.

WORKUP

后处理

  1. customThe title compound was prepared