Dichloromethane → 2-tert-Butoxycarbonylaminopropyl methanesulfonate

HRID 822040Notes

Reaction equation

HRID 822040 reaction equation
[C:1]([CH3:2])([CH3:3])([CH3:4])[O:5][C:6](=[O:7])[NH:8][CH:9]([CH2:10][OH:11])[CH3:12].[CH3:22][S:23]([Cl:24])(=[O:25])=[O:26].[CH:13]([N:14]([CH:15]([CH3:16])[CH3:17])[CH2:18][CH3:19])([CH3:20])[CH3:21].[Cl:27][CH2:28][Cl:29]>>[C:1]([CH3:2])([CH3:3])([CH3:4])[O:5][C:6](=[O:7])[NH:8][CH:9]([CH2:10][O:11][S:23]([CH3:22])(=[O:25])=[O:26])[CH3:12]

Participants

5

Reactant 4

HCID 6344DichloromethaneHCID 31297Methanesulfonyl chlorideHCID 81531DiisopropylethylamineHCID 545701tert-butyl N-(1-hydroxypropan-2-yl)carbamate

Product 1

HCID 144271842-tert-Butoxycarbonylaminopropyl methanesulfonate

Sources & evidence

ORD record
ord-e922f42afb1f45fa8f7fd8ce174fa32c
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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