HRID82229

反应详情

EQUATION

反应方程式

HRID 82229 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

[5-(7-tert-Butyl-7H-pyrrolo[2,3-d]pyrimidine-5-carbonyl)-pyridin-3-yl]-methyl-carbamic acid tert-butyl ester (Example 542) was treated with 4N HCl in Dioxane at room temperature for 2 hours. The solvent was removed in vacuo and the solid obtained was triturated with diethyl ether to afford the title compound as white solid in 100% yield, 76 mg.

WORKUP

后处理

  1. customThe solvent was removed in vacuo
  2. customthe solid obtained
  3. customwas triturated with diethyl ether