HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-N-methoxy-N-methylpyridine-3-carboxamide → HCID 86672126, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-N-methoxy-N-methylpyridine-3-carboxamide | HCID 18472269 | — |
| Reactant | 2-Chloro-5-iodo-7-(2-methoxy-1,1-dimethyl-ethyl)-7H-pyrrolo[2,3-d]pyrimidine | HCID 86672127 | — |
| Product | HCID 86672126 | HCID 86672126 | — |
Reaction Steps
The title compound was prepared according to the method described for Preparation 64 using 2-Chloro-5-iodo-7-(2-methoxy-1,1-dimethyl-ethyl)-7H-pyrrolo[2,3-d]pyrimidine (Preparation 259) and 5-Bromo-N-methoxy-N-methyl-nicotinamide to afford the title compound as yellow gum in 34% yield, 900 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08846698B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-5c84d76bd7d5413e9deedb1ad3b31d94 |
| Source note | uspto-grants-2014_09 |