Dichloromethane → Tert-butyl 2-oxo-2-pyrimidin-2-ylethyl(methyl)carbamate

HRID 826906Notes

Reaction equation

HRID 826906 reaction equation
[C:11]([O:12][CH3:13])([CH3:14])([CH3:15])[CH3:16].[CH2:42]([Cl:43])[Cl:44].[CH3:1][N:2]([C:3]([O:4][C:5]([CH3:6])([CH3:7])[CH3:8])=[O:9])[CH3:10].[CH3:22][O:23][N:24]([C:25](=[O:26])[c:27]1[n:28][cH:29][cH:30][cH:31][n:32]1)[CH3:33].[CH3:34][N:35]([CH3:36])[CH2:37][CH2:38][N:39]([CH3:40])[CH3:41].[CH:17]([Li:18])([CH2:19][CH3:20])[CH3:21]>>[CH2:1]([N:2]([C:3]([O:4][C:5]([CH3:6])([CH3:7])[CH3:8])=[O:9])[CH3:10])[C:25](=[O:26])[c:27]1[n:28][cH:29][cH:30][cH:31][n:32]1

Participants

7

Reactant 6

HCID 6344DichloromethaneHCID 8037N,N,N',N'-TetramethylethylenediamineHCID 15413tert-Butyl methyl etherHCID 312724tert-butyl N,N-dimethylcarbamateHCID 22498726N-Methoxy-N-methylpyrimidine-2-carboxamideHCID 178418400CID 53628100

Product 1

HCID 10285998Tert-butyl 2-oxo-2-pyrimidin-2-ylethyl(methyl)carbamate

Sources & evidence

ORD record
ord-c41146ea016a4049bf01aedca707b9ce
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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