Tetrahydrofuran → 2,3-Dihydro-benzo[b]oxepine-4-carbonylchloride

HRID 830542Notes

Reaction equation

HRID 830542 reaction equation
[O:19]1[CH2:20][CH2:21][CH2:22][CH2:23]1.[O:1]1[c:2]2[c:3]([cH:11][cH:12][cH:13][cH:14]2)[CH:4]=[C:5]([C:8](=[O:9])[OH:10])[CH2:6][CH2:7]1.[S:15]([Cl:16])([Cl:17])=[O:18]>>[O:1]1[c:2]2[c:3]([cH:11][cH:12][cH:13][cH:14]2)[CH:4]=[C:5]([C:8](=[O:9])[Cl:17])[CH2:6][CH2:7]1

Participants

4

Reactant 3

HCID 8028TetrahydrofuranHCID 24386Thionyl ChlorideHCID 11116823HCID 11116823, compound

Product 1

HCID 866497862,3-Dihydro-benzo[b]oxepine-4-carbonylchloride

Sources & evidence

ORD record
ord-8afb26ef16e1495d9b30142c57b0631b
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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