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HRID832

反应详情

EQUATION

反应方程式

HRID 832 的结构方程式

REACTANTS

反应物

3
结构：Cl.NO
HCID443297

未命名化合物

结构：CC(=O)[O-].O.[Na+]
HCID23681166

Sodium acetate hydrate (1:1:1)

C2H5NaO3

结构：C[C@]12CC(=NO)C(=O)C[C@@H]1CC[C@@H]1[C@@H]2CC[C@]2(C)[C@@H](O)CC[C@@H]12
HCID86752163

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)O[C@H]1CC[C@H]2[C@@H]3CC[C@H]4CC(=NO)C(=NO)C[C@]4(C)[C@H]3CC[C@]12C
HCID136395990

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

A suspension of steroid 7, NH2OH.HCl and NaOAc/H2O was refluxed for 20 minutes. The reaction was cooled to room temperature and poured into H2O. The precipitate was collected by filtration. The resulting solid 8 was washed with H2O and air and dried; wt. 23.4 g.

WORKUP

后处理

  1. temperaturewas refluxed for 20 minutes
  2. filtrationThe precipitate was collected by filtration
  3. washThe resulting solid 8 was washed with H2O and air
  4. customdried