反应详情

A flame dried flask was charged with MTBD (0.25 g, 1.63 mmol), ether (10 mL) and a stirbar under dry nitrogen atmosphere. With vigorous stirring a 1M ethereal HCl solution (1.6 mL) was then added to form a white precipitate. Stirring was continued for 1 hour then excess solvent was decanted to yield 0.29 g (94%). The salt was then dried under high vacuum.

1. customA flame dried flask
2. additionwas then added
3. customto form a white precipitate
4. customexcess solvent was decanted
5. customto yield 0.29 g (94%)
6. customThe salt was then dried under high vacuum