HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70619331, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-Methoxyethanol | HCID 8019 | — |
| Reactant | 1-(2-Furoyl)piperazine | HCID 550206 | — |
| Reactant | 5,6-Dimethoxy-1-methyl-1H-benzo[d]imidazole | HCID 754984 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 70619331 | HCID 70619331 | — |
Reaction Steps
3.50 g. 2-chloro. 5,6-dimethoxy-1-methyl benzimidazole [(J. Org. Chem. USSR 1 1466), (1965)] 7.00 g N-(2-furoyl) piperazine, and 25 ml 2-methoxyethanol were reacted as described in Example I. The product was converted to its hydrochloride by dissolving in isopropyl alcohol and acidifying with a solution of HCl gas in isopropyl alcohol. Yield: 3.99 g product, mp 212°-215° C decomp.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04093726 |
| Source dataset | uspto-grants-1978_06 |
| ORD ID | ord-510d2c2837754ab290925241ceab50fa |
| Source note | uspto-grants-1978_06 |