HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86735738, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | n,n-Dimethylpiperazine-1-carboxamide | HCID 712909 | — |
| Reactant | 1-Methoxyethanol | HCID 3015637 | — |
| Reactant | 2-Chloro-5,6-dimethoxy-1H-benzo[d]imidazole | HCID 20325524 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 86735738 | HCID 86735738 | — |
Reaction Steps
3.50 g 2-chloro 5,6-dimethoxybenzimidazole, 7.50 g N,N-dimethyl 1-piperazine carboxamide [J. Org. Chem. 13 144 (1948)], 20 ml methoxyethanol was reacted as described in Example I. The product was converted to the HCl salt with HCl in isopropyl alcohol. Yield: 5.33 g mp 252°-254° C (85%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04093726 |
| Source dataset | uspto-grants-1978_06 |
| ORD ID | ord-3d84d1c841dd4f3db11611c4337f9e5d |
| Source note | uspto-grants-1978_06 |