HuagongsheHuagongshe Chemistry Print Report · For research reference only
Epibromohydrin → 7-(2-Oxiranylmethoxy)-1(2H)-phthalazinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Epibromohydrin | HCID 18430 | — |
| Reactant | HCID 135729098 | HCID 135729098 | — |
| Product | 7-(2-Oxiranylmethoxy)-1(2H)-phthalazinone | HCID 20325496 | — |
Reaction Steps
7-Hydroxy-1(2H)-phthalazinone was reacted with epibromohydrin in a similar manner to that described in Example 1(iii) to give 7-(2,3-epoxypropoxy)-1(2H)-phthalazinone, which after recrystallisation from ethyl acetate had m.p. 164°-166°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04093725 |
| Source dataset | uspto-grants-1978_06 |
| ORD ID | ord-f952617a72b745ca9318e09568c0031a |
| Source note | uspto-grants-1978_06 |