HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 135729098, compound → HCID 135729102, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 135729098 | HCID 135729098 | — |
| Reactant | HCID 135729103 | HCID 135729103 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 135729102 | HCID 135729102 | — |
Reaction Steps
7-Hydroxy-6-nitro-1(2H)-phthalazinone (which may be prepared by the nitration of 7-hydroxy-1(2H)-phthalazinone) is dissolved in aqueous sodium hydroxide, reduced with hydrogen and 10% palladium on charcoal catalyst and the solution filtered and neutralised to give 6-amino-7-hydroxy-1(2H)-phthalazinone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04093725 |
| Source dataset | uspto-grants-1978_06 |
| ORD ID | ord-9d8649fc40904b0293135a4daec96b35 |
| Source note | uspto-grants-1978_06 |