Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 53761679 | HCID 53761679 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 54425803 | HCID 54425803 | — |
Reaction Steps
Combine 6.0 g (16 mmole) of phenyl N-[4-(hexafluoro-2-hydroxy-2-propyl)phenyl]carbamate (Example 12) and 65 ml of NH3 saturated ethanol. After 1/2 hour, pour the reaction mixture into 150 ml of H2O. Concentrate, cool to 0° C and filter off the white solid. Obtain 5.5 g of N-[4-(hexafluoro-2-hydroxy-2-propyl)phenyl]urea; m.p. 181°-183° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04093742 |
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| Source dataset | uspto-grants-1978_06 |
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| ORD ID | ord-51dfe91fa9b34ef28142dd38c0c1f29a |
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| Source note | uspto-grants-1978_06 |
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